Product Note:
The cyclohexanone need not be freshly distilled. Commercial cyclohexanone, obtained from the Barrett Division, Allied Chemical & Dye Corporation, New York, New York, gave practically the same yield as carefully fractionated cyclohexanone.
2. If too much selenous acid is added at once, or the cooling discontinued, the solution will heat up and the reaction will become extremely vigorous with subsequent decrease in yield.
3. Selenous acid or selenium dioxide can apparently be used interchangeably.The cyclohexanone need not be freshly distilled. Commercial cyclohexanone, obtained from the Barrett Division, Allied Chemical & Dye Corporation, New York, New York, gave practically the same yield as carefully fractionated cyclohexanone.
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